• Detection of adulteration in fresh and frozen beefburger products by beef offal using mid-infrared ATR spectroscopy and multivariate data analysis

      Zhao, Ming; Downey, Gerard; O'Donnell, C.P.; Teagasc Walsh Fellowship Programme; Food Safety Authority of Ireland (Elsevier, 17/10/2013)
      A series of authentic and offal-adulterated beefburger samples was produced. Authentic product (36 samples) comprised either only lean meat and fat (higher quality beefburgers) or lean meat, fat, rusk and water (lower quality product). Offal adulterants comprised heart, liver, kidney and lung. Adulterated formulations (46 samples) were produced using a D-optimal experimental design. Fresh and frozen-then-thawed samples were modelled, separately and in combination, by a classification (partial least squares discriminant analysis) and class-modelling (soft independent modelling of class analogy) approach. With the former, 100% correct classification accuracies were obtained separately for fresh and frozen-then-thawed material. Separate class-models for fresh and frozen-then-thawed samples exhibited high sensitivities (0.94 to 1.0) but lower specificities (0.33 – 0.80 for fresh samples and 0.41 – 0.87 for frozen-then-thawed samples). When fresh and frozen-then-thawed samples were modelled together, sensitivity remained 1.0 but specificity ranged from 0.29 to 0.91. Results indicate a role for this technique in monitoring beefburger compliance to label.
    • Food Authentication using Infrared Spectroscopic Methods

      Downey, Gerard; Kelly, J. Daniel (Teagasc, 01/06/2006)
      Confirmation of the authenticity of a food or food ingredient is an increasing challenge for food processors and regulatory authorities. This is especially the case when an added-value claim, such as one relating to geographic origin or a particular processing history, is made on the food label. Regulatory agencies are concerned with the prevention of economic fraud while the food processor needs confirmation of such claims in order to protect a brand, the image of which could be severely damaged should an adulterated ingredient make its way into the branded food product.To be of greatest value, any analytical tool deployed to confirm authenticity claims needs to be portable, easy to use, non-destructive and accurate. Infrared spectroscopy, near and mid-infrared, is a tool which has been demonstrated to possess these properties in a wide range of situations.While some applications in food authenticity have been reported, the work undertaken in this project was designed to explore their capabilities regarding a number of products and authenticity issues of particular interest to the Irish agri-food industry i.e. olive oil, honey, soft fruit purées and apple juice.